A Practical Guide to Supramolecular Chemistry by Peter Cragg

By Peter Cragg

A pragmatic advisor to Supramolecular Chemistry is an introductory guide of sensible experiments for chemists with very little past event of supramolecular chemistry. Syntheses are truly offered to facilitate the practise of acyclic and macrocyclic compounds often encountered in supramolecular chemistry utilizing simple experimental tactics. a number of the compounds can be utilized to demonstrate vintage supramolecular phenomena, for which transparent instructions are given, or could be built extra as a part of the reader's personal learn. The ebook additionally describes suggestions popular within the research of supramolecular behaviour, together with computational equipment, with many particular examples. a useful reference for college kids and researchers within the box embarking on supramolecular chemistry initiatives and searching out a 'tried and established' direction into the chemistry of key compounds. An introductory advisor to functional syntheses concentrating on supramolecular chemistry. absolutely referenced introductions clarify the historic and modern value of every compound Supplementary web site together with 3D molecular constructions, FAQ's approximately syntheses and proposals for extra experiments

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6 [11]. [1] The phthalocyanines, A. B. P. Lever, Adv. Inorg. Chem. , 1965, 7, 27. [2] Template synthesis of macrocyclic compounds, N. V. Gerbeleu, V. B. Arion and J. Burgess, Wiley-VCH, Weinheim, 1999. [3] Industrial applications of phthalocyanines, P. Gregory, J. Porphyrins Phthalocyanines, 2000, 4, 432. [4] Improvements in and relating to the manufacture and use of colouring materials, A. G. Dandridge, H. A. E. Drescher, J. , GB Patent 322169, November 18, 1928. [5] Coordination Compounds of Porphyrins and Phthalocyanines, B.

Stir at 40  C in a 1 L three-necked round-bottomed flask, fitted with a pressureequalized addition funnel and a thermometer, for 30 min. 9 mol) in dry 1,4-dioxane (150 mL) dropwise over 2 h from the addition funnel. During the addition the reaction appears to be slightly exothermic and holds 40  C with minimal external heating. Once all the ditosylate has been added continue to stir for a further 1 h and allow the solution to cool to room temperature. Filter the precipitated sodium tosylate and wash with dichloromethane until the washes are colourless (ca.

Part VI. The structure of the phthalocyanines, C. E. Dent, R. P. Linstead and A. R. Lowe, J. Chem. , 1935, 1033. [7] An X-ray study of the structure of the phthalocyanines. Part I. The metal-free, nickel, copper, and platinum compounds, J. M. Robertson, J. Chem. , 1935, 615, An X-ray study of the phthalocyanines. Part II. Quantitative structure determination of the metalfree compound, J. M. Robertson, J. Chem. , 1936, 1195; An X-ray study of the phthalocyanines. Part III. Quantitative structure determination of nickel phthalocyanine, J.

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