Acceleration And Automation Of Solid Sample Treatment by Garcia J.L.L., de Castro M.D.L.

By Garcia J.L.L., de Castro M.D.L.

This booklet goals to supply scientists with information regarding a sequence of recommendations that may be used with the intention to facilitating the transformation of the pattern to a suitable country for next detection or quantitation of its elements of curiosity. The ideas handled diversity from the extremely simple ones (e.g. freeze-drying) to different extra advanced ones (e.g. glow discharge and laser-induced breakdown sampling).

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Radioanal. , 35 (1978) 161. A. I. P. T. V. M. Byr'ko, Yad. Fiz. Metodv Anal. Kontrole Okruzh. Sredy, 129 (1985) 34. H. D. H. Zoller, Anal. , 129 (1975) 1685. H. Lieser, W. Calmano, E. Heuss and V. Neitzert, J Radioanal. , 37 (1977) 717.

The conditioning of samples for electron microprobe analysis in studies of the soil/root interface [44] or electron microscopy research based on the use of critical drying point to prepare solid samples [45], the extraction of soluble acid phosphates from plants during fixation of the material with liquid nitrogen [46], and the comparison of the performance of thermal processes and freeze-drying as storage methods for food products prior to the determination of metal traces [47], are but a few selected applications that testify to the improvements provided by freeze-drying the sample prior to the determination of inorganic species.

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